Kjeldahl determination of nitrogen in vegetable soil

Soil nitrogen is one of the important signs of soil fertility and an important nutrient for crop growth. The total nitrogen content and the existence of the species closely relate to the growth of the crop. Therefore, the accurate determination of soil total nitrogen and other forms of nitrogen content is the evaluation standard for soil fertility. The Kjeldahl method is generally used for the determination of soil total nitrogen, that is, Kjeldahl nitrogen analyzer is used for effective inspection and analysis.

The total nitrogen in the soil boils liquid to distillation, and the traditional tracking distillation unit uses glass half. With the development of modern instruments, Kjeldahl is widely accepted in various laboratories for the determination of feed protein, total soil nitrogen, etc. Kjeldahl can be automatically distilled, automatically titrated, or manually completed. The effect of manual and automatic is the same, which can greatly shorten the total nitrogen determination time, save time and labor, and save time and labor to determine the analysis and expression of the uncertainty of soil total nitrogen in vegetables.

At room temperature, after the sample is digested with potassium permanganate, the nitrite nitrogen in the sample is oxidized to nitrate nitrogen, and then all the nitrate nitrogen is converted into the niobium nitrogen by using the reduced iron powder. Finally, the sample is used. The temperature-controlled digester, under the participation of accelerator selenium powder and copper sulfate-potassium sulfate, was digested with concentrated sulfuric acid, and various nitrogen-containing organic compounds were decomposed at high temperature, and all were converted into the niobium nitrogen chart. The cooking solution was automatically distilled and titrated with a Kjeldahl apparatus to calculate the total nitrogen content of the soil.

Using the Kjeldahl nitrogen analyzer to determine the soil nitrogen content in vegetable fields, temperature-controlled digesters can be used in place of traditional digesters, making it easier to adjust the temperature. The Kjeldahl meter titrates well-digested samples, making the process quick and easy. Through the test of this sample, it can be found that the Kjeldahl tester has good reproducibility of the test, and the entire digestion, distillation and titration detection process can fully meet the test requirements of the test standard, and the result is accurate and reasonable.

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